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L-tert-Leucine
ethyl trifluoroacetate,
N-trifluoroacetyl tert-leucine
| Conditions | Yield |
|---|---|
|
With
potassium methanolate;
In
methanol;
at 40 ℃;
for 2h;
|
N-trifluoroacetyl tert-leucine
methylamine
N'-trifluoroacetyl-S-tert-leucine N-methylamide
| Conditions | Yield |
|---|---|
|
N-trifluoroacetyl tert-leucine;
With
Vilsmeier reagent;
In
ethyl acetate;
at -15 ℃;
for 2h;
methylamine;
In
water; ethyl acetate;
|
39.0 g |
L-tert-Leucine
ethyl trifluoroacetate,
(1R,2S,5S)-N-{(1R)-1-cyano-2-[(3S)-2-oxopyrrolidin-3-yl]ethyl}-6,6-dimethyl-3-[3-methyl-N-(trifluoroacetyl)-L-valyl]-3-azabicyclo[3.1.0]hexane-2-carboxamide
(1R,2S,5S)-N-{(1S)-1-cyano-2-[(3S)-2-oxopyrrolidin-3-yl]ethyl}-6,6-dimethyl-3-[3-methyl-N-(trifluoroacetyl)-L-valyl]-3-azabicyclo[3.1.0]hexane-2-carboxamide
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