74927-72-3

  • Product Name(R)-(-)-N-(3,5-Dinitrobenzoyl)-alpha-phenylglycine
  • Molecular FormulaC15H11N3O7
  • Molecular Weight345.268
  • Purity99%
  • Appearancewhite to light yellow crystal powder
Inquiry

Product Details

Quick Details

  • CasNo: 74927-72-3
  • Molecular Formula: C15H11N3O7
  • Appearance: white to light yellow crystal powder
  • Purity: 99%

Top Purity (R)-(-)-N-(3,5-Dinitrobenzoyl)-alpha-phenylglycine 74927-72-3 In Bulk Supply

  • Molecular Formula:C15H11N3O7
  • Molecular Weight:345.268
  • Appearance/Colour:white to light yellow crystal powder 
  • Vapor Pressure:8.34E-14mmHg at 25°C 
  • Melting Point:217-218 ºC 
  • Refractive Index:-102 ° (C=1, THF) 
  • Boiling Point:569.4 °C at 760 mmHg 
  • Flash Point:298.2 °C 
  • PSA:158.04000 
  • Density:1.527 g/cm3 
  • LogP:3.49600 

(R)-(-)-N-(3,5-DINITROBENZOYL)-ALPHA-PHENYLGLYCINE(Cas 74927-72-3) Usage

Chemical Properties

white to light yellow crystal powde

Uses

(R)-(-)-N-(3,5-Dinitrobenzoyl)-alpha-phenylglycine

InChI:InChI=1/C15H11N3O7/c19-14(16-13(15(20)21)9-4-2-1-3-5-9)10-6-11(17(22)23)8-12(7-10)18(24)25/h1-8,13H,(H,16,19)(H,20,21)/t13-/m1/s1

74927-72-3 Relevant articles

Chiral High-Pressure Liquid Chromatographic Stationary Phases. 3. General Resolution of Arylalkylcarbinols

Pirkle, William H.,Finn, John M.

, p. 2935 - 2938 (1981)

Enantiomers of arylalkylcarbinols (1) ma...

COMPOSITIONS AND METHODS FOR CYCLOFRUCTANS AS SEPARATION AGENTS

-

Page/Page column 48, (2010/12/31)

The present invention relates to derivat...

Development of new HPLC chiral stationary phases based on native and derivatized cyclofructans

Sun, Ping,Wang, Chunlei,Breitbach, Zachary S.,Zhang, Ying,Armstrong, Daniel W.

experimental part, p. 10215 - 10226 (2010/05/01)

An unusual class of chiral selectors, cy...

Continuous separation of racemic 3,5-dinitrobenzoyl-amino acids in a centrifugal contact separator with the aid of cinchona-based chiral host compounds

Hallett, Andrew J.,Kwant, Gerard J.,De Vries, Johannes G.

supporting information; experimental part, p. 2111 - 2120 (2009/09/30)

The resolution of racemates is mostly pe...

Chiral permselectivity in nanoporous opal films surface-modified with chiral selector moieties

Cichelli, Julie,Zharov, Ilya

, p. 1870 - 1875 (2008/02/07)

The chiral permselectivity in thin opal ...

74927-72-3 Process route

(R)-phenylglycine
875-74-1

(R)-phenylglycine

3,5-dinitrobenoyl chloride
99-33-2

3,5-dinitrobenoyl chloride

(R)-(-)-N-(3,5-dinitrobenzoyl)-α-phenylglycine
74927-72-3

(R)-(-)-N-(3,5-dinitrobenzoyl)-α-phenylglycine

Conditions
Conditions Yield
In tetrahydrofuran; at 20 ℃; for 168000h;
92%
In tetrahydrofuran; Yield given; Ambient temperature; 7-10 days;
(R,S)-N-(3,5-dinitrobenzoyl)-phenylglycine methyl ester

(R,S)-N-(3,5-dinitrobenzoyl)-phenylglycine methyl ester

(R)-(-)-methyl N-(3,5-dinitrobenzoyl)-α-phenylglycinate
69632-50-4

(R)-(-)-methyl N-(3,5-dinitrobenzoyl)-α-phenylglycinate

(S)-(+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine
90761-62-9

(S)-(+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine

(R)-(-)-N-(3,5-dinitrobenzoyl)-α-phenylglycine
74927-72-3

(R)-(-)-N-(3,5-dinitrobenzoyl)-α-phenylglycine

(S)-(+)-methyl N-(3,5-dinitrobenzoyl)-α-phenylglycinate

(S)-(+)-methyl N-(3,5-dinitrobenzoyl)-α-phenylglycinate

Conditions
Conditions Yield
With sodium hydroxide; N-pivaloyl-(3,5-dimethylphenyl)-L-prolinamide; In tetrachloromethane; dichloromethane; water; at 0 ℃; Title compound not separated from byproducts.;

74927-72-3 Upstream products

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    875-74-1

    (R)-phenylglycine

  • 99-33-2
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    3,5-dinitrobenoyl chloride

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    phenylglycin

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    (R)-(-)-N-(3,5-dinitrobenzoyl)-α-phenylglycine

74927-72-3 Downstream products

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    (R)-(-)-methyl N-(3,5-dinitrobenzoyl)-α-phenylglycinate

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    1222074-04-5

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    (3S)-7-bromo-2,3-dihydro-1-benzofuran-3-aminium (2R)-{[(3,5-dinitrophenyl)carbonyl]amino}(phenyl)ethanoate

;

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