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6-bromo-4,4-dimethyl-2,3-dihydrothiochromene is a member of the thiochromene family of compounds, which are known for their biological and pharmacological activities. This particular compound has a bromine atom and two methyl groups attached to a six-membered ring containing a sulfur atom and an oxygen atom. Its properties make it useful in organic synthesis and medicinal chemistry.
InChI:InChI=1/C11H13BrS/c1-11(2)5-6-13-10-4-3-8(12)7-9(10)11/h3-4,7H,5-6H2,1-2H3
We report a general preparation of aryla...
The addition of nucleophilic organometal...
A Br?nsted acid-catalyzed 1,4-addition h...
One-pot synthesis of 6-bromo-4,4-dimethy...
1-Bromo-4-(3-methylbut-2-enylsulphanyl)benzene
6-bromo-4,4-dimethyl-3,4-dihydro-2H-1-benzothiopyran
| Conditions | Yield |
|---|---|
|
With polyphosphoric acid; In toluene; at 100 ℃; for 48h; Inert atmosphere;
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86% |
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With polyphosphoric acid; In toluene; at 100 ℃; for 48h; Inert atmosphere; Sealed tube;
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53% |
|
With phosphorus pentaoxide; methanesulfonic acid;
|
|
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With methanesulfonic acid; phosphorus pentoxide; at 20 ℃; for 2h;
|
|
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With phosphorus pentoxide; In methanesulfonic acid; at 20 ℃; for 2h;
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![1-bromo-4-[(3-methylbut-3-en-1-yl)sulfanyl]benzene](/upload/2023/6/2765fba4-79c9-4357-a300-1964a5d03cbd.png)
1-bromo-4-[(3-methylbut-3-en-1-yl)sulfanyl]benzene
6-bromo-4,4-dimethyl-3,4-dihydro-2H-1-benzothiopyran
| Conditions | Yield |
|---|---|
|
With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 2h;
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1-Bromo-4-(3-methylbut-2-enylsulphanyl)benzene
4,4-dimethyl-3,4-dihydro-2H-1-benzothiopyran
1-bromo-4-[(3-methylbut-3-en-1-yl)sulfanyl]benzene
para-bromobenzenethiol
tazarotene
4,4-dimethyl-6-(phenylthio)thiochromane
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