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We have designed and synthesised a new o...
![methyl (S)-2-benzyloxycarbonylamino-3-[4-(2-t-butoxycarbonylaminoethoxy)phenyl]propionate](/upload/2023/6/94a7041d-f7e6-454e-9969-8347c99cda88.png)
methyl (S)-2-benzyloxycarbonylamino-3-[4-(2-t-butoxycarbonylaminoethoxy)phenyl]propionate
2-amino-3-[4-(2-tert-butoxycarbonylamino-ethoxy)-phenyl]-propionic acid methyl ester
| Conditions | Yield |
|---|---|
|
With
ammonium formate;
palladium on activated charcoal;
In
methanol;
at 25 ℃;
for 3h;
|
N-(benzyloxycarbonyl)-L-tyrosine methyl ester
2-amino-3-[4-(2-tert-butoxycarbonylamino-ethoxy)-phenyl]-propionic acid methyl ester
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 2 steps
1: 73 percent / PPh3; DEAD / tetrahydrofuran; toluene / 48 h / 25 °C
2: ammonium formate / Pd/C / methanol / 3 h / 25 °C
With
ammonium formate; triphenylphosphine; diethylazodicarboxylate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; toluene;
1: Mitsunobu reaction;
|
methyl (S)-2-benzyloxycarbonylamino-3-[4-(2-t-butoxycarbonylaminoethoxy)phenyl]propionate
2-(N-tert-butoxycarbonylamino)ethanol
N-(benzyloxycarbonyl)-L-tyrosine methyl ester
2-(2-benzyloxycarbonylamino-ethylamino)-3-[4-(2-tert-butoxycarbonylamino-ethoxy)-phenyl]-propionic acid methyl ester
2-{(2-benzyloxycarbonylamino-ethyl)-[(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-3-[4-(2-tert-butoxycarbonylamino-ethoxy)-phenyl]-propionic acid methyl ester
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