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Product Details
Chemical Properties |
white to off-white fine crystalline powder |
Uses |
Protected (S) enantiomer of the amino acid Phenylalanine. |
InChI:InChI=1/C10H13NO2/c1-13-10(12)9(11)7-8-5-3-2-4-6-8/h2-6,9H,7,11H2,1H3/p+1/t9-/m0/s1
Two different types of new phosphinamide...
The invention provides application of a ...
New C2 symmetric chiral diimines were sy...
Elaborate fragments of the proposed ster...
2-methyl-propan-1-ol
(S)-N-acetylphenylalanine
2-methylpropyl acetate
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride
Conditions | Yield |
---|---|
(S)-N-acetylphenylalanine;
With
triphenyl phosphite; chlorine; triethylamine;
In
tetrahydrofuran;
at -30 ℃;
2-methyl-propan-1-ol;
In
tetrahydrofuran;
at -30 - 20 ℃;
With
water;
|
95% |
L-phenylalanine
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride
Conditions | Yield |
---|---|
With
thionyl chloride;
In
methanol;
|
100% |
With
thionyl chloride;
In
methanol;
at 0 - 20 ℃;
|
100% |
With
thionyl chloride;
In
methanol;
|
98% |
With
thionyl chloride;
In
methanol; diethyl ether;
|
95% |
In
methanol; benzene;
for 4h;
Ambient temperature;
|
42% |
With
hydrogenchloride;
|
|
Multi-step reaction with 2 steps
1: thionyl chloride
With
thionyl chloride;
|
|
With
hydrogenchloride; methanol;
In
di-isopropyl ether;
at 55 ℃;
for 0.0833333h;
Heating / reflux;
|
|
With
thionyl chloride;
In
methanol;
|
|
With
hydrogenchloride;
In
methanol; toluene;
|
methanol
L-phenylalanine
N-formyl-L-phenylalanine
DL-β-chloro-β-phenylalanine hydrochloride
2?(1,3?dioxoisoindolin?2?yl)acetyl methyl phenylalaninate
(S)-2-(nicotinamido)-3-phenylpropanoic acid
methyl N-trityl-(S)-phenylalaninate
N-benzyloxycarbonylglycyl-L-phenylalanine methyl ester
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